malvern mastersizer 2000 user manual pdf
To search measurement files: 1. Description and Features.3 2. Web3 Mastersizer 2000 User Manual MAN0384 Issue 1.0 March 2007. Always adopt the correct procedures for disposing of the sample and dispersant, following any local guidelines. It is a measure of the amount of laser light lost due to the introduction of the sample into the analyser beam. 5.1.3 Switch on the computer and start the software by double click on the Mastersizer Malvern 2000 Icon on the desktop. Select Configure-Existing SOP. When the Options button in the Measurement Display is pressed, the Measurement Options dialogue appears. Sea cual sea su situacin, Malvern le proporcionar el soporte tcnico adecuado para usted. Many dialogues also have Advice buttons, giving more general advice. To delete an SOP: 1. For example, selecting the Measured on header lists all records into numeric Measured on date order. Cell The cell is the interface between the sample dispersion unit and the optical bench. While stirring, continually fill and empty the pipette. Page 8-10 MAN 0384, 107 9 Advanced features Introduction This chapter covers features experienced users can use to improve their analyses: Obscuration settings limits can be set, enabling the system to detect poor conditions and take action if a limit is exceeded. 3. Mastersizer 2000 Page 5-3, 66 Chapter 5 Viewing the results Changing the Records tab By default the Records tab displays seven fields which include Record number, Sample name, Source, Measured on, etc. Malvern Mastersizer 2000 Manuals Mastersizer 2000 Page 9-3, 110 Chapter 9 Advanced features Obscuration filtering Obscuration filtering rejects data that does not fall within the set limits. If passwords are not set up, the user just has to type their username to log in, otherwise they must provide the password too. The software records the number of snaps measured and this figure can be used in reports to indicate the completeness of a measurement. Proceed as described above for adding a user. Malvern Instruments makes every effort to ensure that this document is correct. A user can change the properties of the record by selecting it then using Edit- Result editor. We are currently located in Cameroon. This describes the amount of absorption that takes place as the light enters the particle. This will allow you to create an icon for easy access to your virtual desktop. Operator An operator is a person trained to use the instrument. For example an obscuration of 30% means that 30% of the analyser beam has been lost by either scattering or absorption. Representative sampling. Calculated quality parameter. Use the command File-Send, which opens the computer s default mail program, and attach the file. Mastersizer 2000 Page 5-9, 72 Chapter 5 Viewing the results Page 5-10 MAN 0384, 73 6 Understanding the views Introduction This chapter gives guidelines on the interpretation of the results from the Mastersizer. Clicking on the Sample handling unit list box displays a list of available samplers. Page 8-2 MAN 0384, 99 Sample preparation Chapter 8 Representative sampling When taking a sample for a measurement, it is vital to ensure that the sample used is representative of the whole sample. Supervisors skilled users who can perform configuration and create SOPs. Sorting records Records in a measurement file can be sorted into alphanumeric order. Security guidelines. Instructions, 20 Manor Road Ruislip Middlesex HA4 7LB Telephone: +44(0)1895 624 774 E-Mail: info@llmedia.com Website: www.llmedia.com Instructions for the ACER Laptops Always, after connecting to a projector, switch, User Manual Dual Laser InfraRed (IR) Thermometer with Color Alert MODEL 42509 Introduction Congratulations on your purchase of the Model 42509 IR Thermometer with Color Alert. D PRODUCTIVITY THROUGH INNOVATION 600 CONTROL DIRECT DRIVE TECHNICAL/OPERATION MANUAL 10 BORIGHT AVENUE, KENILWORTH NEW JERSEY 07033 TELEPHONE: 800-524-0273 FAX: 908-686-9317 TABLE OF CONTENTS Page, Overview Why Bluetooth? Grade efficiency grade efficiency curves created from particle sizing results are used to establish the efficiency of separators such as hydrocyclones, sedimenting centrifuges or gravitational clarifiers. The average will be created as a separate new measurement record capable of being saved and recalled. The measurement is now complete. Making a basic SOP measurement Start an SOP by selecting Measure-Start SOP. Select Measure-Manual. Optical models This section contrasts the Fraunhofer approximation used in some instruments with the Mie theory which underpins Mastersizer 2000 operation. The system measures how much sample is added by monitoring the obscuration of the beam caused by the sample being added to the dispersant. Mastersizer 2000 laboratory equipment pdf manual download. Autosampler 2000 manual The Autosampler 2000 has its own manual giving details on its use. The first record must be set as the reference by selecting it, then right-clicking and selecting Set reference result. The peak of the frequency curve gives the modal diameter, the most commonly occurring particle diameter. Laser Diffraction Masterclass: Why do you Need Material Optical Properties? The Report Designer is detailed in Chapter 5. The capturing of the scattering pattern from the prepared sample - this is known as the measurement. 9. 6. Below is a list of these people and their responsibility: Malvern personnel Malvern personnel (service engineers, representatives, etc.) Mastersizer 2000 Page 7-1, 90 7 Chapter 7 Records and files Handling measurement files The fundamental unit of storage is the record. Select ADD. Permissions are the access rights that are allowed for each user group; these range from the right to edit SOPs to the right to disable view selection. NETGEAR, Inc. 4500 Great America Parkway Santa Clara, CA 95054 USA 208-10060-01 2006-03-17, Internet Explorer 7. The Ultrasonic support removal tank automatically removes PLA support material from a printed ABS, Page 1 Centran Version 4 Getting Started Guide KABA MAS Kaba Mas Welcome Kaba Mas, part of the world-wide Kaba group, is the world's leading manufacturer and supplier of high security, electronic safe, 4-Port Pocket USB KVM Switch with USB 2.0 Hub Manual - 1 - Index 1. Copyright 2023 - Malvern Panalytical Ltd is a. User Manual, Greenline Industrial Monitors IMD-C Series. Click OK. For simplicity, in general text the term Mastersizer 2000 refers to both the Mastersizer 2000 and 2000E. For users who have never operated a Malvern particle analyser before, we recommend reading this manual fully before starting the first measurement. A representative sample must be taken. In most cases the difference is small but the geometric mean is chosen in these calculations as more appropriate to the logarithmic spacing of the fundamental size classes. Spreadsheet Software BCS ITQ Level 2. This will restore the box to the full range. A fresh sample that has not had time to absorb moisture from the atmosphere is always preferable and usually gives better results. Dmn [, ] = m 3 V i d i n 3 V i d i m n Page 6-4 MAN 0384, 77 Understanding the views Chapter 6 D(v, 0.5), D(v, 0.1) and D(v, 0.9) are standard percentile readings from the analysis. Changing an item s properties Set the properties of any added element by selecting it and double-clicking to open the Properties dialogue(s). Can save inconvenience. WebThis manual includes a system overview,. To define a size band manually: 1. Selecting the header of the field, dragging the header off the page and then releasing the mouse button. See Chapter 9 for more details. Contact the United Kingdom help desk if the local Malvern representative is not available. Web the mastersizer 3000 is the worlds leading particle size analyzer for accurate and rapid particle size measurements. The links below will allow your organization to claim its place in the hierarchy of Kansas Citys premier businesses, non-profit organizations and related organizations. Targus Wireless Remote Presenter USER S GUIDE. Sign in or Register to comment. A typical Measurement window is shown below. For example, by reading the values from the graph (right-hand axis) the user may be able to determine that 10% of the sample is under 23 microns. EigenLight S500 Power Monitor Software Manual Software Installation 1 Installing S500 Power Monitor Software and LabVIEW Run-time Engine 1 Install Drivers for Windows XP 4 Install VISA run-time View the Best Practices in Poster Design located at http://www.emich.edu/training/poster before you begin creating a poster. When a user logs on If security is configured users are prompted for a password when they try to log in: If the administrator selected the User Must Change Password at Next Logon check box (see above), the user sees this dialogue when they log in: To change the user password, the user has to enter the current password and specify a new password with confirmation. To transform a result in an SOP measurement: 1. The supervisor can perform all user maintenance routines identified in the Essentials Manual, including changing the fuses. The statistics of the distribution are calculated from the results using the derived diameters D[m,n] - an internationally agreed method of defining the mean and other moments of particle size. Generally a computer monitor displays information in a landscape format while a printer prints in a portrait format. When asked to confirm deletion of the file, select Yes. To do this, obtain a suitable sample to measure and a suitable dispersant to disperse it in. The target obscuration values can be set by the user; see Chapter 9. Select the Enable transformation check box and select the relevant Transform Volume to radio button. The sample should be correctly mixed before a measurement is taken. Making a basic SOP measurement Start an SOP by selecting Measure-Start SOP. It gives an indication of how well the optical properties for the material were described. To overcome this, the Mastersizer takes many snapshots (known as snaps) and averages the result. 6. To remove any result range reduction press the Default button. Then in PowerPoint: (A) set up the poster size and orientation, (B) add and, Using Microsoft Word Many Word documents will require elements that were created in programs other than Word, such as the picture to the right. Once the correct amount of sample has been added, press the Start button to start the actual measurement. 21 CFR Part 11 support enhanced (when 21CFR Part 11 Key installed). how much ultrasonic dispersion is required? Difficulty in obtaining low background despite many rinses. A table or graph can be dragged and dropped into another application by selecting the item, then dragging while holding the Ctrl key. When the dispersant has been added to the dispersion unit and circulated, we advise switching off the unit briefly to allow trapped air to escape the system. It also allows the user to specify options regarding the result calculation. If the sample/dispersant used is not normally removed with a single flush, enter a number in the Flush cycles box to run the flush sequence that number of times. 4. Guidelines Use a maximum obscuration of about 5% for dry measurements (or even lower for fine dry material). In case a totally inappropriate feed rate is set, so that the obscuration seldom (if ever) falls within the desired limits, a time-out is provided to allow the user to exit the measurement. Mastersizer 2000 Some samples can only be measured in a dry state as they react with all wet dispersants, for example they may dissolve or the particles may swell when in contact with a liquid. To get the most benefit from this chapter we advise reading it once, then reading it a second time while following the instructions to make a measurement. Selecting the legend check box places a summary table, showing date and name, at the foot of each graph. Add Sample this tab shows how much sample has been added to the tank for measurement. Ingrams industry ranking lists are your go-to source for knowing the most influential companies across dozens of business sectors. Specify the SOP file to save the changes to as a new SOP. Alignment alarms In normal operation the alignment of the system is monitored by the software and an auto-alignment procedure is automatically performed if the system is out of alignment. For systems plumbed into the mains supplies a small header tank may overcome this problem. The result-under plot is calculated from the initial size bands by fitting a curve to the analysis data so that values within a size band can be read. Chapter 6 gives details on interpreting the information in a report. Overview SMART Bridgit software is a client/server application that lets you share programs and information with anyone, anywhere in the world. Pressing OK changes the security settings. COMPUTER connector The RS232 cable from the computer is plugged in here. Beware of using a magnetic stirrer to mix a liquid sample. Malvern Mastersizer 2000 This user manual is a companion to the Mastersizer 2000 Essentials Manual which gives Health and Safety, maintenance and other vital information which all users must read. Remember that, if the sample is poorly prepared (unrepresentative or badly dispersed) then the basic data will be incorrect; no amount of analysis of this data will give a correct answer. To edit an SOP: 1. Add enough sample (add one drop at a time) to make the blue Laser Obscuration bar show green (try and achieve a mid value). Measuring new samples: manual measurement The basic procedure is the same as the demonstration outlined above. The measure background facility makes a measurement of the system with only clean dispersant in as well as a measurement of the electrical background. Instead, hold the container in both hands and gently roll the container, continually changing its orientation for about 20 seconds. English, March 2007 ill 7760 Mastersizer 2000 Page 4-25, 62 Chapter 4 Making measurements - a tutorial Quantities dialogue Use this dialogue to define the quantities of sample/additives to be added during a measurement. In a typical SOP measurement there are only a few things the user has to do: Page 4-10 MAN 0384, 47 Making measurements - a tutorial Chapter 4 1. Whenever difficulties in dispersion are experienced, consider using another dispersant. BEFORE USING THE UNIT READ THESE INSTRUCTIONS FULLY AND RETAIN THEM FOR FUTURE REFERENCE, User Manual Dual Laser InfraRed (IR) Thermometer MODEL 42512 Introduction Congratulations on your purchase of the Model 42512 IR Thermometer. Manual sample dispersion unit for Mastersizer 2000 Pressing the Clear button removes all entries in the List of User Sizes list box. In performing this calculation the representative diameter for each band is taken to be the geometric mean of the size band limits: This number will be slightly different to the arithmetic mean: For example, the size band microns has a geometric mean of microns and an arithmetic mean of microns. 5. Mastersizer2000. In a new system, adding Decon 90 to the tank overnight and rinsing 7 or 8 times will wet out the cell surface and reduce bubble formation. This is particularly important for users who are also transforming the result, where small modes in the volume distribution, caused by errors, are magnified and can become dominant when transformed to a number distribution. As an example, a user may have previously used sieve measurements to control a process and may now want to replace the sieves with the Mastersizer. This facility is particularly useful where the sample concentration is liable to some degree of fluctuation, as with some dry powder measurements. To re-analyse a record: 1. Drain The drain allows any spillages within the cell area to exit onto the bench. Statistics shows the mean, standard deviation, maximum and minimum of a group of selected measurement records. For the Mastersizer 2000E the Hydro 2000MU. We have 1 Malvern Mastersizer 2000 manual available for free PDF download: User Manual Malvern Mastersizer 2000 User Manual (154 pages) Brand: Malvern | Category: Laboratory Equipment | Size: 8.07 MB Installation this gives enough information to allow the user, for example, to move the system from one laboratory to another. All help topics can be accessed through the standard help screen by selecting Help- Help topics. Add surfactant or admixture or use ultrasonic action. Integrated systems for particle sizing. Pump clean dispersant through the cell using the pump and stirrer controls on the dispersion unit, before starting the measurement. Model 407780. If a blue refractive index is not given, the Mastersizer assumes that it has the same value as the red refractive index. As a practical demonstration, consider a cement manufacturer who is asked to measure a sample from the production line every hour for five hours. Never try to lift the optical bench by this handle. The tubing must be connected correctly. Also see the section on bubbles later in this chapter. Malvern Mastersizer 2000 Operation & users manual (154 pages) Dry powders, for example, tend to separate out if stored for some time or vibrated. Symptoms of poor sample preparation. Stop this button stops the current measurement process. Protection window The protection window stops dust and dirt entering and damaging the internal detectors. Independent 25, Keyboard Shortcuts Instead of the Mouse Tape 1--4:00 RADAR is a windows based product. Material dialogue This dialogue has two sections, Optical properties and Result calculation: Optical properties Use this section to define the optical properties of the material measured. Select a tab and change any of the entries as required. Large particles tend to move to the outside of the container due to centrifugal separation, and this can lead to sample biasing. For example Page 4-6 MAN 0384, 43 Making measurements - a tutorial Chapter 4 an obscuration of 30% means that 30% of the analyser beam has been lost by either scattering or absorption. The software will automatically make an electrical and optical background measurement as well as aligning the optics. 3. An SOP can be created in one laboratory and then distributed to all Mastersizer 2000 users within an organisation. Select OK to add the search criterion to the list box in the previous dialogue. Rapidly increasing obscuration. A reference record must first be selected. The basics of making a measurement There are two ways to make a measurement: Using a Standard Operating Procedure (SOP) SOPs are user defined procedures that are easily programmed into the software to allow the same type of sample to be measured in a consistent way with all the difficult decisions on measurement strategy already having been made. 2. Select the Alarms button in the Advanced options section. Start starts a measurement process. Introduction. Mastersizer 2000 Page 4-11, 48 Chapter 4 Making measurements - a tutorial Making a basic manual measurement To make a manual measurement select Measure-Manual. Specific Surface Area (SSA) the total area of the particles divided by the total weight. Select OK the changes will be saved.
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